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The mechanical activation was carried out using a laboratory Fritsh planetary ball mill (Model: P7) using stainless vials and balls with a diameter of 12 mm, up to 70 h.A total of 15 g powder was used in all milling runs.The ball-to-powder weight ratio was maintained as 4:3 and the milling speed was adjusted to 600 rpm.The selected milling sequence was 15 min of …

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